農(nóng)藥獸藥多組分殘留質(zhì)譜分析技術(shù)：第2卷.獸藥

Main Researchers/Editors xxvii
Preface xxix
Brief Introduction xxxi

1. Sulfonamides 1
1.1 Curative Effects and Side Effects of Sulfonamides 1
1.2 Chemical Structures and Maximum Residue Limits for Sulfonamide Drugs 2
1.3 Determination of 16 Sulfonamide Residues in Livestock and Poultry Muscles—LC-MS-MS Method (GB/T 20759-2006) 8
1.3.1 Scope 8
1.3.2 Principle 8
1.3.3 Reagents and Materials 8
1.3.4 Apparatus 9
1.3.5 Sample Pretreatment 9
1.3.6 Determination 9
1.3.7 Precision 10
1.3.8 Recovery 12
Researchers 12
Further Reading 16
1.4 Determination of 16 Sulfonamide Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22966-2008) 16
1.4.1 Scope 16
1.4.2 Principle 16
1.4.3 Reagents and Materials 17
1.4.4 Apparatus 17
1.4.5 Sample Pretreatment 18
1.4.6 Determination 18
1.4.7 Precision 19
1.4.8 Recovery 28
Researchers 28
1.5 Determination of 18 Sulfonamide Residues in Fugu and Eel—LC-MS-MS Method (GB/T 22951-2008) 29
1.5.1 Scope 29
1.5.2 Principle 29
1.5.3 Reagents and Materials 29
1.5.4 Apparatus 30
1.5.5 Sample Pretreatment 31
1.5.6 Determination 31
1.5.7 Precision 35
1.5.8 Recovery 36
Researchers 40
1.6 Determination of 8 Sulfonamides residues in Honey—LC-FLD Method (GB/T 18932.5-2002) 41
1.6.1 Scope 41
1.6.2 Principle 41
1.6.3 Reagents and Materials 41
1.6.4 Apparatus 42
1.6.5 Sample Pretreatment 42
1.6.6 Determination 43
1.6.7 Precision 43
1.6.8 Recovery 46
Researchers 47
Further Reading 47
1.7 Determination of 16 Sulfonamide Residues in Honey—LC-MS-MS Method (GB/T 18932.17-2003) 47
1.7.1 Scope 47
1.7.2 Principle 47
1.7.3 Reagents and Materials 48
1.7.4 Apparatus 48
1.7.5 Sample Pretreatment 48
1.7.6 Determination 49
1.7.7 Precision 52
1.7.8 Recovery 52
Researchers 55
Further Reading 55
1.8 Determination of 18 Sulfonamide Residues in Royal Jelly—LC-MS-MS Method (GB/T 22947-2008) 56
1.8.1 Scope 56
1.8.2 Principle 56
1.8.3 Reagents and Materials 56
1.8.4 Apparatus 57
1.8.5 Sample Pretreatment 58
1.8.6 Determination 58
1.8.7 Precision 62
1.8.8 Recovery 64
Researchers 66

2. β-Adrenoceptor Agonists 67
2.1 Determination of 12 β-Agonist Residues in Milk and Milk Powder—LC-MS-MS Method (GB/T 22965-2008) 67
2.1.1 Scope 67
2.1.2 Principle 67
2.1.3 Reagents and Materials 68
2.1.4 Apparatus 69
2.1.5 Sample Pretreatment 69
2.1.6 Determination 70
2.1.7 Precision 76
2.1.8 Recovery 76
Researchers 78
Further Reading 78
2.2 Determination of 12 β-Agonist Residues in Fugu, Eel,and Baked Eel—LC-MS-MS Method (GB/T 22950-2008) 81
2.2.1 Scope 81
2.2.2 Principle 81
2.2.3 Reagents and Materials 81
2.2.4 Apparatus 82
2.2.5 Sample Pretreatment 83
2.2.6 Determination 84
2.2.7 Precision 85
2.2.8 Recovery 85
Researchers 85
Further Reading 88

3. Aminoglycoside 91
3.1 Curative Effects and Side Effects of Streptomycin 91
3.2 Chemical Structures and Maximum Residue Limits for Streptomycin and Dihydrostreptomycin 92
3.3 Determination of Streptomycin Residues in Honey—LC-FLD (GB/T 18932.3-2002) 93
3.3.1 Scope 93
3.3.2 Principle 93
3.3.3 Reagents and Materials 93
3.3.4 Apparatus 94
3.3.5 Sample Pretreatment 95
3.3.6 Determination 95
3.3.7 Precision 97
3.3.8 Recovery 97
Researchers 97
Further Reading 97
3.4 Determination of Streptomycin, Dihydrostreptomycin,and Kanamycin Residues in Milk and Milk
Powder—LC-MS-MS Method (GB/T 22969-2008) 98
3.4.1 Scope 98
3.4.2 Principle 98
3.4.3 Reagents and Materials 98
3.4.4 Apparatus 99
3.4.5 Preparation and Storage of Test Sample 100
3.4.6 Determination 101
3.4.7 Precision 104
3.4.8 Recovery 104
Researchers 105