物理化學實驗指導（二版）

第一部分 緒論(Part One Introduction)
一、物理化學實驗的目的和要求
二、物理化學實驗的安全知識
三、物理化學實驗的設(shè)計思想
四、誤差理論和有效數(shù)字
五、實驗數(shù)據(jù)的表示法和處理
1．Objective and requirement
2．Physical chemistry laboratory safety
3．Rules for designing of the physical chemistry experiment
4．Error theory and significant figures
5．Data reporting
第二部分 實驗(Part Two Experjments)
實驗一 燃燒熱的測定
Experiment 1 Heats Of Combustion
實驗二 溶解熱的測定
Expenment 2 Heats of Solution
實驗三 凝固點降低法測定摩爾質(zhì)量和滲透壓
Experiment 3 Molar Mass and Osmotic：Pressure by Freezing Point Depression
實驗四 液體飽和蒸氣壓的測定
Expenment 4 Saturated Vapor Pressure of Pure LJquids
實驗五 反應平衡常數(shù)及分配系數(shù)的測定
Expenment 5 Equilibrium Constant 0f Reaction and PaItitiml Coefficient
實驗六 完全互溶雙液系平衡相圖的繪制
Expenment 6 Phase Diagram of a Miscible Binary Liquid Svstem
實驗七 雙組分簡單低共熔體系相圖的繪制
Expenment 7 Solid-liquid Binary Phase Diagram
實驗八 三組分液-液系統(tǒng)相圖的繪制
Experiment 8 A Ternary Phase Diagram for a System of Three Liquids
實驗九 電解質(zhì)水溶液電導的測定及應用
Experiment 9 Measurement and Application of Electrolyte Solution
Conductance
實驗十 電動勢法測溶液pH和反應熱力學函數(shù)
Experiment 10 Determinations of pH of Solution and Thermodynamic Functions
by Electromotive Force Measurements
實驗十一 一級反應速率常數(shù)的測定
Experiment 11 Rate Constant for First Order Reaction
實驗十二 碘化鉀與過氧化氫反應的速率常數(shù)及活化能的測定
Experiment 12 Kinetics of Reaction between Potassium Iodide and Hydrogen
Peroxide
實驗十三 丙酮溴化反應速率常數(shù)的測定
Experiment 13 Rate Constant and Activation Energy of the Bromination of
Acetone
實驗十四 乙酸乙酯皂化反應速率常數(shù)及活化能的測定
Experiment 14 Rate Constant for the Saponification of Ethyl Acetate by
Conductometric Method
實驗十五 最大泡壓法測定溶液的表面張力
Experiment 15 Surface Tension of Solutions by Bubble Pressure Method
實驗十六 固體在溶液中的吸附
Experiment 16 Adsorption of Solids in Solution
實驗十七 乳狀液的制備和性質(zhì)
Experiment 17 Preparation and Properties of Emulsion
實驗十八 溶膠的制備及性質(zhì)
Experiment 18 Preparation and Properties of Sols
實驗十九 黏度法測定大分子的平均相對分子質(zhì)量
Experiment 19 Average Relative Molar Mass of the Macromolecule by
Viscosity Method
實驗二十 納米材料的合成與表征(綜合設(shè)計性試驗)
Experiment 20 Preparation and Characterization of Nanomaterials
(Multi—designing Experiment)
實驗二十一 藥物穩(wěn)定性及有效期測定(設(shè)計性實驗)
Experiment 21 Determination of Drug Stability and Shelf Life
(Designing Experiment)
實驗二十二 固體藥物常規(guī)理化常數(shù)的測定(綜合設(shè)計性實驗)
Experiment 22 Physical and Chemical Constants of Drugs
(Multi—designing Experiment)
附錄(Appendices)
常用物理化學數(shù)據(jù)表(Reference Data of Experimental Physical Chemistry)
參考文獻(References)